HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Mesylphenylacetic acid → HCID 70975807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Mesylphenylacetic acid | HCID 572345 | — |
| Reactant | HCID 70976345 | HCID 70976345 | — |
| Product | HCID 70975807 | HCID 70975807 | — |
Reaction Steps
The product from Example 57B and 2-(4-(methylsulfonyl)phenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ 11.78 (s, 1H), 8.34 (dd, J=7.9, 1.1, 1H), 8.08 (d, J=7.7, 1H), 8.03-7.97 (m, 1H), 7.97-7.92 (m, 1H), 7.92-7.87 (m, 2H), 7.60 (d, J=8.3, 2H), 7.45-7.40 (m, 2H), 7.40-7.30 (m, 3H), 3.81 (s, 2H), 3.22 (s, 3H); MS (APCI+) M/Z 466 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859549B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-5ea4ebef675d49fea04bf3d542a39681 |
| Source note | uspto-grants-2014_10 |