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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 535600Generated: October 29, 2026

4-Mesylphenylacetic acid → HCID 70975807, compound

https://huagongshe.com/reaction/535600

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Mesylphenylacetic acidHCID 572345—
ReactantHCID 70976345HCID 70976345—
ProductHCID 70975807HCID 70975807—

Reaction Steps

The product from Example 57B and 2-(4-(methylsulfonyl)phenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ 11.78 (s, 1H), 8.34 (dd, J=7.9, 1.1, 1H), 8.08 (d, J=7.7, 1H), 8.03-7.97 (m, 1H), 7.97-7.92 (m, 1H), 7.92-7.87 (m, 2H), 7.60 (d, J=8.3, 2H), 7.45-7.40 (m, 2H), 7.40-7.30 (m, 3H), 3.81 (s, 2H), 3.22 (s, 3H); MS (APCI+) M/Z 466 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08859549B2
Source datasetuspto-grants-2014_10
ORD IDord-5ea4ebef675d49fea04bf3d542a39681
Source noteuspto-grants-2014_10