HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Mesylphenylacetic acid → HCID 70975944, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Mesylphenylacetic acid | HCID 572345 | — |
| Reactant | HCID 70975871 | HCID 70975871 | — |
| Product | HCID 70975944 | HCID 70975944 | — |
Reaction Steps
The product from Example 68B and 2-(4-(methylsulfonyl)phenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ 11.97 (s, 1H), 8.56 (d, J=8.2, 1H), 8.42-8.35 (m, 1H), 8.15-8.08 (m, 1H), 8.04-7.99 (m, 3H), 7.91 (d, J=8.3, 2H), 7.82-7.77 (m, 1H), 7.71-7.65 (m, 2H), 7.57 (d, J=8.3, 2H), 3.83 (s, 2H), 3.24 (s, 3H); MS (DCI+) M/Z 515 (M+NH4)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859549B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-a3f2f195ffe54739977e0bb87889c3c6 |
| Source note | uspto-grants-2014_10 |