4-Chlorophenylacetyl chloride → HCID 70976215, compound

Participants

Reaction Steps

The product from Example 195B and 2-(4-chlorophenyl)acetyl chloride were processed using a method similar to that described in Example 4C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ 11.70 (s, 1H), 8.34 (d, J=7.1, 1H), 8.08-8.03 (m, 1H), 8.03-7.98 (m, 1H), 7.97-7.92 (m, 1H), 7.56 (d, J=8.6, 2H), 7.44-7.36 (m, 4H), 7.35-7.31 (m, 2H), 3.67 (s, 2H); MS (DCI+) M/Z 519 (M+NH4)+.

Provenance & Evidence