HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Trifluoromethyl)benzeneacetic acid → HCID 70975994, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Trifluoromethyl)benzeneacetic acid | HCID 67695 | — |
| Reactant | HCID 70975871 | HCID 70975871 | — |
| Product | HCID 70975994 | HCID 70975994 | — |
Reaction Steps
The product from Example 68B and 2-(3-(trifluoromethyl)phenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.93-11.95 (bs, 1H), 8.55-8.57 (m, 1H), 8.37-8.40 (m, 1H), 8.09-8.13 (m, 1H), 7.98-8.03 (m, 3H), 7.77-7.82 (m, 1H), 7.59-7.71 (m, 6H), 3.83 (s, 2H); MS (ESI−) M/Z 486 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859549B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-9e5fafd4811c4edcb276bf9f550a8beb |
| Source note | uspto-grants-2014_10 |