HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluorophenylacetic acid → HCID 70975777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluorophenylacetic acid | HCID 145424 | — |
| Reactant | HCID 70976123 | HCID 70976123 | — |
| Product | HCID 70975777 | HCID 70975777 | — |
Reaction Steps
The product from Example 212B and (3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.75 (s, 1H), 8.32-8.35 (m, 1H), 7.91-8.02 (m, 3H), 7.39-7.41 (m, 2H), 7.24-7.27 (m, 3H), 7.14-7.18 (m, 3H), 4.34 (s, 2H), 3.79 (s, 2H); MS (DCI+) M/Z 455 (M+NH4)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859549B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-67723092555e46f19e15507bc65a5969 |
| Source note | uspto-grants-2014_10 |