4-Chlorophenylacetyl chloride → HCID 70976214, compound

Participants

Reaction Steps

The product from Example 212B and (4-chlorophenyl)acetyl chloride were processed using a method similar to that described in Example 4C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.69 (s, 1H), 8.32 (dd, J=8.1, 1.3 Hz, 1H), 7.90-8.01 (m, 3H), 7.37-7.43 (m, 6H), 7.23-7.26 (m, 3H), 4.32 (s, 2H), 3.72 (s, 2H); MS (DCI+) M/Z 453 (M+NH4)+.

Provenance & Evidence