HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-5-chloro-2-methyl-3-nitrobenzene → 3-Bromo-5-chloro-2-methylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-5-chloro-2-methyl-3-nitrobenzene | HCID 24728096 | — |
| Reactant | 2-Chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine | HCID 58164432 | — |
| Product | 3-Bromo-5-chloro-2-methylaniline | HCID 53429593 | — |
Reaction Steps
This material was prepared from 1-bromo-5-chloro-2-methyl-3-nitrobenzene following the procedure used for SM-9, step 3 (96%): LCMS (m/z): 219.9 (MH+); tR=0.99 minute.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859548B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-6ad08fe813334864b4a896634c4f1128 |
| Source note | uspto-grants-2014_10 |