HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → 4-[(3-Chloropropyl)sulfonyl]morpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 3-Chloropropanesulphonyl chloride | HCID 15410 | — |
| Product | 4-[(3-Chloropropyl)sulfonyl]morpholine | HCID 284407 | — |
Reaction Steps
The procedure used for the preparation of Intermediate D was used to prepare the title compound from 3-chloropropanesulfonyl chloride and morpholine. High vacuum drying gave the title compound (1.3 g, 104%): 1H NMR (CDCl3) δ: 2.20-2.29 (2H, m), 3.02 (2H, dd), 3.20-3.23 (4H, m), 3.64 (2H, t), 3.68-3.72 (4H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859572B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-47c6a6ed53a64a11afce7f2f6206aa6b |
| Source note | uspto-grants-2014_10 |