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HRID536226

反应详情

EQUATION

反应方程式

HRID 536226 的结构方程式

REACTANTS

反应物

2
结构：CNC
HCID674

Dimethylamine

C2H7N

结构：O=S(=O)(Cl)CCCCl
HCID15410

Propanesulfonyl chloride, chloro-

C3H6Cl2O2S

PRODUCTS

生成物

1
结构：CN(C)S(=O)(=O)CCCCl
HCID10035328

3-chloro-N,N-dimethylpropane-1-sulfonamide

C5H12ClNO2S

PROCEDURE

实验过程

The procedure used for the preparation of Intermediate D was used to prepare the title compound from 3-chloropropanesulfonyl chloride and dimethylamine. High vacuum drying gave the title compound (2.1 g, 100%): 1H NMR (DMSO-d6) δ: 2.06-2.11 (2H, m), 2.75 (6H, s), 3.10-3.15 (2H, m), 3.72 (2H, t).