HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 3-chloro-N,N-dimethylpropane-1-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 3-Chloropropanesulphonyl chloride | HCID 15410 | — |
| Product | 3-chloro-N,N-dimethylpropane-1-sulfonamide | HCID 10035328 | — |
Reaction Steps
The procedure used for the preparation of Intermediate D was used to prepare the title compound from 3-chloropropanesulfonyl chloride and dimethylamine. High vacuum drying gave the title compound (2.1 g, 100%): 1H NMR (DMSO-d6) δ: 2.06-2.11 (2H, m), 2.75 (6H, s), 3.10-3.15 (2H, m), 3.72 (2H, t).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859572B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-6752174e0ffa469aa497eeb1583e1dba |
| Source note | uspto-grants-2014_10 |