Diethylamine → HCID 10262652, compound

HRID 536227Notes

Reaction equation

[Cl:1][CH2:2][CH2:3][CH2:4][S:5](Cl)(=[O:7])=[O:6].[CH2:9]([NH:11][CH2:12][CH3:13])[CH3:10]>>[Cl:1][CH2:2][CH2:3][CH2:4][S:5]([N:11]([CH2:12][CH3:13])[CH2:9][CH3:10])(=[O:7])=[O:6]

Participants

Reactant 2

HCID 8021Diethylamine

HCID 154103-Chloropropanesulphonyl chloride

Product 1

HCID 10262652HCID 10262652, compound

Procedure

The procedure used for the preparation of Intermediate D was used to prepare the title compound from 3-chloropropanesulfonyl chloride and diethylamine. High vacuum drying gave the title compound (570 mg, 95%) which was used without characterization in the next step.

Sources & evidence

ORD record: ord-e744fa13332941118e62522db7368c88
Source dataset: uspto-grants-2014_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08859572B2

Reaction notes

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