Cyanuric chloride → 4-(4,6-Dichloro-1,3,5-triazin-2-yl)-3,5-dimethylmorpholine

HRID 536879Notes

Reaction equation

[N:1]1[C:8]([Cl:9])=[N:7][C:5](Cl)=[N:4][C:2]=1[Cl:3].[CH3:10][CH:11]1[CH2:16][O:15][CH2:14][CH:13]([CH3:17])[NH:12]1>>[Cl:9][C:8]1[N:1]=[C:2]([Cl:3])[N:4]=[C:5]([N:12]2[CH:13]([CH3:17])[CH2:14][O:15][CH2:16][CH:11]2[CH3:10])[N:7]=1

Participants

Reactant 2

HCID 7954Cyanuric chloride

HCID 88623,5-Dimethylmorpholine

Product 1

HCID 866365254-(4,6-Dichloro-1,3,5-triazin-2-yl)-3,5-dimethylmorpholineYield 35%

Procedure

The title compound was prepared by following the procedure of Example 462 step 3 using cyanuric chloride and 3,5-dimethylmorpholine. Yield 5 g, 35% yield.

Sources & evidence

ORD record: ord-a36f6a4706394b5f9f94a26475cd014f
Source dataset: uspto-grants-2014_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08859542B2

Reaction notes

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