HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57496383, compound → 2-Cyclohexyl-4-phenylpiperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57496383 | HCID 57496383 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Cyclohexyl-4-phenylpiperidine | HCID 57496384 | — |
Reaction Steps
Benzyl 2-cyclohexyl-4-phenyl-3,6-dihydropyridine-1(2H)-carboxylate (4.7 g, 12.52 mmol) in EtOH (25 ml) was added Pd/C (1.18 g, 0.554 mmol) and hydrogenated with a balloon for 10 hours. Filter through celite and concentrate. The crude piperidine was not purified. LRMS (M+H)=217.10
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08865701B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-984b5586a16248c49f6b387ecf0a9861 |
| Source note | uspto-grants-2014_10 |