HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Difluoro-3-hydroxybenzamide → HCID 46237271, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Difluoro-3-hydroxybenzamide | HCID 45120136 | — |
| Reactant | 2-Chloromethyl-6-methoxybenzothiazole | HCID 59402709 | — |
| Product | HCID 46237271 | HCID 46237271 | 19% |
Reaction Steps
Synthesised from 2,6-difluoro-3-hydroxybenzenecarboxamide and 2-(chloromethyl)-6-methoxy-1,3-benzothiazole according to Method B, scheme 2. Yield 19%, mp 190-192° C., HPLC-MS (method 1): m/z 351 [M+H]+, Rt=3.50 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08865736B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-101c757e9bbe49e5a2a610ea02fcc589 |
| Source note | uspto-grants-2014_10 |