Methyl 2-methylbutyrate → HCID 66616447, compound

HRID 538718Notes

Reaction equation

HRID 538718 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[C:6](Cl)=O.[CH3:14][CH:15]([CH2:20][CH3:21])[C:16](OC)=[O:17].O.[NH2:23][NH2:24]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C:6]2[C:15]([CH2:20][CH3:21])([CH3:14])[C:16](=[O:17])[NH:23][N:24]=2)[CH:9]=[CH:10][C:11]=1[O:12][CH3:13]

Participants

4

Reactant 3

HCID 13357Methyl 2-methylbutyrateHCID 24654Hydrazine hydrate (1:1)HCID 77070Veratroyl chloride

Product 1

HCID 66616447HCID 66616447, compound

Procedure

Prepared analogously as described for example C5 using 3,4-dimethoxybenzoyl chloride, methyl 2-methylbutanoate and hydrazine hydrate as starting compounds.

Workup

  1. customPrepared analogously

Sources & evidence

ORD record
ord-27e2f1f21fad4b29ab6ccfded8f8f451
Source dataset
uspto-grants-2014_10
Patent number
US08865745B2

Reaction notes

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