HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 57476519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | (4-Bromo-3-methylphenyl)methanol | HCID 10987288 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57476519 | HCID 57476519 | — |
Reaction Steps
A solution of compound 2 (2.0 g, 9.95 mmol), Et3N (6.94 mL, 49.7 mmol), and CH2Cl2 (100 mL) was cooled to 0° C. and treated with methanesulfonyl chloride (1.54 mL, 19.9 mmol). The solution was stirred at room temperature for 3 hours. The volatiles were removed under reduced pressure and the resultant crude product was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08865914B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-99ecd2b1c796419f93e846b7ecfb79a7 |
| Source note | uspto-grants-2014_10 |