HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methanesulfonyl chloride → 2-Azidopentyl methanesulfonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methanesulfonyl chloride | HCID 31297 | — |
| Edukt | 5-Azidopentanol | HCID 10866358 | — |
| Edukt | 2-Azidoethyl methanesulfonate | HCID 11275197 | — |
| Produkt | 2-Azidopentyl methanesulfonate | HCID 86675085 | — |
Reaktionsschritte
Reaction of 5-azidopentanol (1.1 g, 8.53 mmol) and mesyl chloride (0.98 mL, 12.79 mmol) within 3 h as described for synthesis of 156a gave compound 156d (1.54 g) as a crude colorless oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08871728B2 |
| Quelldatensatz | uspto-grants-2014_10 |
| ORD ID | ord-d946bfd704e0410b9c55cbe4321e77ed |
| Quellennotiz | uspto-grants-2014_10 |