HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-hydrazinyl-N,N-dimethyl-2-oxoacetamide → HCID 178424710, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-hydrazinyl-N,N-dimethyl-2-oxoacetamide | HCID 43164112 | — |
| Reactant | 2-(Tetrahydrofuran-3-yl)acetohydrazide | HCID 68288816 | — |
| Reactant | 4-(1-(2,4-dimethyl-5-(5-((tetrahydrofuran-3-yl)methyl)-4H-1,2,4-triazol-3-yl)benzoyl)piperidin-4-yl)benzonitrile | HCID 178424704 | — |
| Product | HCID 178424710 | HCID 178424710 | — |
Reaction Steps
The title compound was prepared using standard chemical manipulations and procedures similar to those used for the preparation of 4-(1-(2,4-dimethyl-5-(5-((tetrahydrofuran-3-yl)methyl)-4H-1,2,4-triazol-3-yl)benzoyl)piperidin-4-yl)benzonitrile (compound 130), using 2-hydrazinyl-N,N-dimethyl-2-oxoacetamide (compound 135.1) instead of 2-(tetrahydrofuran-3-yl)acetohydrazide (compound 130.4). m/z (ES+) 457 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871790B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-ff1781e95cba4ed6b37c3679dbda8d93 |
| Source note | uspto-grants-2014_10 |