HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19961156, compound → 5,6-Dihydroxy-1-(N-methyl)aminomethyl-3-phenyl-3,4-dihydronaphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19961156 | HCID 19961156 | — |
| Reactant | 1-Aminomethyl-5,6-dimethoxy-3-phenyl-3,4-dihydronaphthalene | HCID 19961157 | — |
| Product | 5,6-Dihydroxy-1-(N-methyl)aminomethyl-3-phenyl-3,4-dihydronaphthalene | HCID 19961196 | — |
Reaction Steps
1-Aminomethyl-5,6-dimethoxy-3-phenyl-3,4-dihydronaphthalene, the product of Step 2 of Example 2, was N-methylated as described in Example 111 and deprotected as described in Step 4 of Example 2 to give the title compound as its hydrochloride salt, m.p. 131°-133° C.; DCI MS: 282 (M+H)+. Analysis calculated for C18H20ClNO2 : C, 68.03; H, 6.34; N, 4.41. Found: C, 67.64; H, 6.54; N, 4.31.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05621133 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-1b22fb7e0867494b88b4a5016bacffc8 |
| Source note | uspto-grants-1997_04 |