HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-1H-imidazole-5-carbonyl chloride hydrochloride → HCID 69017448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-1H-imidazole-5-carbonyl chloride hydrochloride | HCID 2776553 | — |
| Reactant | 6-Chloro-2,4,8,22-tetraazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaen-11-amine bis(trifluoroacetate) | HCID 86636255 | — |
| Product | HCID 69017448 | HCID 69017448 | 29% |
Reaction Steps
The desired compound was prepared according to the procedure of Example B26, using 6-chloro-2,4,8,22-tetraazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaen-11-amine bis(trifluoroacetate) and 1-methyl-1H-imidazole-5-carbonyl chloride hydrochloride as the starting materials in 29% yield. LCMS for C23H21ClN7O (M+H)+: m/z=446.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871753B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-aed57b6bb4b7431e97b73c14a010e462 |
| Source note | uspto-grants-2014_10 |