HuagongsheHuagongshe Chemistry Print Report · For research reference only
Picolinoyl Chloride Hydrochloride → HCID 57962706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Picolinoyl Chloride Hydrochloride | HCID 135033 | — |
| Reactant | HCID 57961661 | HCID 57961661 | — |
| Product | HCID 57962706 | HCID 57962706 | 29% |
Reaction Steps
The desired compound was prepared as a white powder according to the procedure of Example C22, step F, using 6-chloro-2,4,8,14,22-pentaazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaene and pyridine-2-carbonyl chloride hydrochloride as the starting materials in 29% yield. LCMS for C23H18ClN6O (M+H)+: m/z=429.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871753B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-8f7842438e5f4180a8413a6f3173ff1b |
| Source note | uspto-grants-2014_10 |