HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenacyl bromide → HCID 13882925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178469144 | HCID 178469144 | — |
| Product | HCID 13882925 | HCID 13882925 | 65.4% |
Reaction Steps
Reaction of product of Example 35 with bromoacetophenone and potassium carbonate similar to the above Example 63 gave a crude product which was recrystallized successively from methanol and cyclohexane to give 4.45 g (65.4%) of product as a solid; mp 95°-97° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04655816 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-5de37b0cdc6b4ef9bdafc5dce0731437 |
| Source note | uspto-grants-1987_04 |