HRID542195

反应详情

EQUATION

反应方程式

HRID 542195 的结构方程式

PROCEDURE

实验过程

0.01 mole (2.65 g) of 1-[bis(hydroxymethyl)-methyl]-6,7-dimethoxy-3,4-dihydroisoquinoline is boiled with 10 ml of a 46% hydrogen bromide solution for 4 hours. The mixture is evaporated and the residue is triturated with acetone to yield the aimed compound.

WORKUP

后处理

  1. customThe mixture is evaporated
  2. customthe residue is triturated with acetone