HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → 6-(Aminomethyl)pyridin-2(1H)-one hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | (6-Methoxypyridin-2-yl)methanamine | HCID 13882973 | — |
| Product | 6-(Aminomethyl)pyridin-2(1H)-one hydrobromide | HCID 13563589 | — |
Reaction Steps
The crude product from Example 2 was combined with 10 ml of 48% hydrobromic acid, and the resulting mixture was heated at its reflux temperature for one hour. Evaporation to dryness provided 6-aminomethyl-2(1H)-pyridone hydrobromide as a water-soluble solid. The structural assignment was supported by infrared and nuclear magnetic resonance spectral analyses.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04656285 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-1a9f767402184eff825e95da8669c952 |
| Source note | uspto-grants-1987_04 |