HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylamide → Methyl 2-hydroxy-2-(1-oxo-2-propenylamino)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylamide | HCID 6579 | — |
| Reactant | Phenothiazine | HCID 7108 | — |
| Reactant | Pyruvate | HCID 107735 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Methyl 2-hydroxy-2-(1-oxo-2-propenylamino)acetate | HCID 157058 | — |
Reaction Steps
Acrylamide (141.7 parts), methylglyoxylate (144 parts), acetone (1200 ml) and phenothiazine (0.05 parts) were mixed and heated to reflux for 6 hours. After filtration and crystallization 180 parts MAG were received as confirmed by chemical analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04656308 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-de147820d35d48f790e3e830afb93185 |
| Source note | uspto-grants-1987_04 |