huagongshe.com
HRID542334

反应详情

EQUATION

反应方程式

HRID 542334 的结构方程式

REACTANTS

反应物

3
结构：C=CC(N)=O
HCID6579

Acrylamide

C3H5NO

结构：c1ccc2c(c1)Nc1ccccc1S2
HCID7108

Phenothiazine

C12H9NS

结构：CC(=O)C(=O)[O-]
HCID107735

Pyruvate

C3H3O3-

PRODUCTS

生成物

1
结构：C=CC(=O)NC(O)C(=O)OC
HCID157058

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

Acrylamide (141.7 parts), methylglyoxylate (144 parts), acetone (1200 ml) and phenothiazine (0.05 parts) were mixed and heated to reflux for 6 hours. After filtration and crystallization 180 parts MAG were received as confirmed by chemical analysis.

WORKUP

后处理

  1. temperatureheated
  2. temperatureto reflux for 6 hours
  3. filtrationAfter filtration and crystallization 180 parts MAG