HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → methyl (2RS, 3S)-3-amino-2-hydroxy-5-methylhexanoate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | (2RS,3S)-3-amino-2-hydroxy-5-methylhexanoic acid | HCID 12879199 | — |
| Product | methyl (2RS, 3S)-3-amino-2-hydroxy-5-methylhexanoate hydrochloride | HCID 13746619 | — |
Reaction Steps
Hydrogen chloride was passed into a solution 110 mg of (2RS, 3S)-3-amino-2-hydroxy-5-methylhexanoic acid in 10 ml of methanol under ice-cooling, and the mixture was stirred overnight. The reaction mixture was evaporated to dryness under reduced pressure to obtain 150 mg of methyl (2RS, 3S)-3-amino-2-hydroxy-5-methylhexanoate hydrochloride as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04656269 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-1c24ddd1af8940dd8558ad7229b1883a |
| Source note | uspto-grants-1987_04 |