HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-aminoethyl)acetamide → HCID 13853582, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-aminoethyl)acetamide | HCID 66082 | — |
| Reactant | 5-(4-Isocyanatophenyl)pyrazin-2(1H)-one | HCID 20208661 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13853582 | HCID 13853582 | — |
Reaction Steps
In a manner similar to Example 13b, 5-[4-(isocyanato)phenyl]-2(1H)-pyrazinone is reacted with 2-acetamidoethylamine (1 g) in dimethylformamide (5 ml) for 17 hours at room temperature to form the title compound, m.p. 238°-44° C.; δ(DMSO-d6) 1.80 (s, 3H, COCH3), 7.94, 8.08 (2s, 2H, pyrazinone H's).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04657906 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-e5cf6e6893fe40e1bddee6f60ee1a7e3 |
| Source note | uspto-grants-1987_04 |