HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13672378, compound → HCID 178526257, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13672378 | HCID 13672378 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178526257 | HCID 178526257 | 57.5% |
Reaction Steps
In this example, 4-benzyloxy-2-(11-hydroxyundecyl) quinoline-N-oxide is dissolved in methanol and catalytically reduced with a catalyst of 10% palladium-carbon under the atmospheric pressure. Then, the catalyst is removed therefrom by filtration, and the solvent is also removed therefrom by distillation. The residue is recrystallized from ethanol, whereby the cationed compound is obtained (yield: 57.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04657916 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-e37e2f3136804670a716b2399ca4f50f |
| Source note | uspto-grants-1987_04 |