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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 542695Generated: October 31, 2026

Potassium Carbonate → HCID 54312464, compound

https://huagongshe.com/reaction/542695

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant1-IodohexaneHCID 12527—
ReactantHCID 136023524HCID 136023524—
SolventDimethylformamideHCID 6228—
ProductHCID 54312464HCID 54312464—

Reaction Conditions

Temperature80 °C

Reaction Steps

A mixture of 15.3 g of 2-(2-p-hydroxyphenyl-5-pyridyl)-thiophene, 6.9 g of K2CO3, 25 g of hexyl iodide and 250 ml of DMF is heated at 80° C. for 16 hours, with stirring, and then cooled and worked up in the customary manner. 2-(2-p-Hexoxyphenyl-5-pyridyl)-thiophene is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04659503
Source datasetuspto-grants-1987_04
ORD IDord-36c9e6bea95d4b378578d5a7fca00fcf
Source noteuspto-grants-1987_04