HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → HCID 13769980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 13769978 | HCID 13769978 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 13769980 | HCID 13769980 | — |
Reaction Steps
Chloroacetyl chloride (1.9 ml) is added in 20 minutes, contemporaneously with triethylamine (3.4 ml), to a suspension of 4,9-dihydro-10H-pyrido[3,2-b]thieno[3,2-e][1,4]-diazepin-10-one (4.4 g) in dioxane (200 ml), heated to reflux.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04659707 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-ecaf327baa9145f0a57716ea68f35666 |
| Source note | uspto-grants-1987_04 |