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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 542723Generated: October 25, 2026

Ammonium Hydroxide → 3-acetyl-8-methoxy-7-sulfamoyl-2,3,4,5-tetrahydro-1H-3-benzazepine

https://huagongshe.com/reaction/542723

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmonium HydroxideHCID 14923—
Reactant3-acetyl-7-chlorosulfonyl-8-methoxy-2,3,4,5-tetrahydro-1H-3-benzazepineHCID 13853350—
Product3-acetyl-8-methoxy-7-sulfamoyl-2,3,4,5-tetrahydro-1H-3-benzazepineHCID 13853351—

Reaction Steps

3-Acetyl-7-chlorosulfonyl-8-methoxy-2,3,4,5-tetrahydro-1H-3-benzazepine (3 g, 0.007 m) was treated with concentrated ammonium hydroxide (10 ml), stirred for 2 hours and filtered to give 3-acetyl-8-methoxy-7-sulfamoyl-2,3,4,5-tetrahydro-1H-3-benzazepine, m.p. 260°-263°.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04659706
Source datasetuspto-grants-1987_04
ORD IDord-82bbe709232a4491a3065977726b067f
Source noteuspto-grants-1987_04