HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetoacetate → HCID 13826845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 1-Benzothiophene-3-carbaldehyde | HCID 227328 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13826845 | HCID 13826845 | — |
Reaction Steps
Following the procedure of Example 1B, 2.04 g of benzo[b]thiophene-3-carboxaldehyde, 3.2 ml of ethyl acetoacetate, and 1.5 ml of ammonium hydroxide were allowed to react in 15 ml of ethanol to provide 1.4 g of the desired title product, m.p. 139°-142° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04659717 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-c5eab1ec46694fc19a12d33dd0925dd1 |
| Source note | uspto-grants-1987_04 |