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HRID542784

反应详情

EQUATION

反应方程式

HRID 542784 的结构方程式

REACTANTS

反应物

2
结构：c1ccc(CNCc2ccccc2)cc1
HCID7656

Dibenzylamine

C14H15N

结构：ClCC1CO1
HCID7835

Epichlorohydrin

C3H5ClO

PRODUCTS

生成物

1
结构：OC(CCl)CN(Cc1ccccc1)Cc1ccccc1
HCID13535479

未命名化合物

收率 70%

PROCEDURE

实验过程

4.93 g (0.25 mol) of dibenzylamine and 25.4 g (0.275 mol) of epichlorohydrin are stirred for 3 hours under nitrogen at 85° to 90° C. The golden yellow oil obtained is distilled under a high vacuum. 50.5 g (70%) of a colourless oil are obtained.

WORKUP

后处理

  1. customThe golden yellow oil obtained
  2. distillationis distilled under a high vacuum