Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Piperidine → 1-methyl-3-(1-methyl-1H-tetrazol-5-yl)-7-piperidino-4-quinolone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Piperidine | HCID 8082 | — |
| 반응물 | 7-fluoro-1-methyl-3-(1-methyl-1H-tetrazol-5-yl)-4-quinolone | HCID 13474453 | — |
| 생성물 | 1-methyl-3-(1-methyl-1H-tetrazol-5-yl)-7-piperidino-4-quinolone | HCID 13474431 | — |
반응 단계
A mixture of 7-fluoro-1-methyl-3-(1-methyl-1H-tetrazol-5-yl)-4-quinolone (0.2 g) and piperidine (5 ml) was heated on a steam bath for 22 hours. The mixture was cooled and the solid product was collected and recrystallised from industrial methylated spirit to give the novel compound 1-methyl-3-(1-methyl-1H-tetrazol-5-yl)-7-piperidino-4-quinolone, m.p. 180°-183°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04659718 |
| 출처 데이터셋 | uspto-grants-1987_04 |
| ORD ID | ord-a57b66c102c341d0b4434e2b4dfb88c2 |
| 출처 메모 | uspto-grants-1987_04 |