HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20207845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,2,4-Tris(2-oxiranylmethyl)-1,2,4-triazolidine-3,5-dione | HCID 71218 | — |
| Solvent | Sodium Chloride | HCID 5234 | — |
| Product | HCID 20207845 | HCID 20207845 | — |
Reaction Steps
A total of 36.5 g of 10% hydrochloric acid was added dropwise at 40° C. to a solution of 26.9 g (0.1 mole) of 1,2,4-triglycidyl urazole (TGU) in 700 ml of 10% aqueous sodium chloride solution so slowly that the pH-value could be kept constant at pH 5. The addition was over after about 70 minutes. Thereafter the reaction mixture was extracted 4 times with 250 ml of methylene chloride and the methylene chloride distilled off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04659824 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-96fbddc4dc8147c6be58e6b4c12d1b49 |
| Source note | uspto-grants-1987_04 |