Hydrochloric Acid → HCID 20207845, compound

HRID 542928Notes

Reaction equation

HRID 542928 reaction equation
[ClH:1].[CH2:2]([N:6]1[C:11](=[O:12])[N:10]([CH2:13][CH:14]2[O:16][CH2:15]2)[C:8](=[O:9])[N:7]1[CH2:17][CH:18]1[O:20][CH2:19]1)[CH:3]1[O:5][CH2:4]1>[Cl-].[Na+]>[CH2:2]([N:6]1[C:11](=[O:12])[N:10]([CH2:13][CH:14]([OH:16])[CH2:15][Cl:1])[C:8](=[O:9])[N:7]1[CH2:17][CH:18]1[O:20][CH2:19]1)[CH:3]1[O:5][CH2:4]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 712181,2,4-Tris[(oxiran-2-yl)methyl]-1,2,4-triazolidine-3,5-dione

Product 1

HCID 20207845HCID 20207845, compound

Reagents, catalysts & solvents 1

HCID 5234Sodium ChlorideSolvent

Procedure

A total of 36.5 g of 10% hydrochloric acid was added dropwise at 40° C. to a solution of 26.9 g (0.1 mole) of 1,2,4-triglycidyl urazole (TGU) in 700 ml of 10% aqueous sodium chloride solution so slowly that the pH-value could be kept constant at pH 5. The addition was over after about 70 minutes. Thereafter the reaction mixture was extracted 4 times with 250 ml of methylene chloride and the methylene chloride distilled off.

Workup

  1. additionThe addition
  2. customafter about 70 minutes
  3. extractionThereafter the reaction mixture was extracted 4 times with 250 ml of methylene chloride
  4. distillationthe methylene chloride distilled off

Sources & evidence

ORD record
ord-96fbddc4dc8147c6be58e6b4c12d1b49
Source dataset
uspto-grants-1987_04
Patent number
US04659824

Reaction notes

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