Sodium Fluoride → HCID 20207847, compound

Participants

Reaction Steps

2.1 g (50 mMoles of sodium fluoride were added to a solution of 1.5 g (5 mMoles) of 1,2-diglycidyl-4-(3-chloro-2-hydroxypropyl)-urazole in 100 ml of acetone and the mixture boiled for 6 hours. After the solvent had been distilled off and the residue taken up in 50 ml of methylene chloride, followed by filtration, removal of the methylene chloride by distillation and drying in an oil pump vacuum at 40° C., 1,2-diglycidyl-4-(3-fluoro-2-hydroxypropyl)-urazole, refractive index nD20 :1.4955 (colorless liquid), was obtained in a yield of 1.5 g (100%).

Provenance & Evidence