HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic acid, [4-(hexylamino)-4-oxobutyl]methyl-, phenylmethyl ester → HCID 20206870, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic acid, [4-(hexylamino)-4-oxobutyl]methyl-, phenylmethyl ester | HCID 20206828 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20206870 | HCID 20206870 | — |
Reaction Steps
A solution of the 4-(N-benzyloxycarbonyl-N-methylamino)-N-n-hexylbutyramide thus obtained (6.6 g.) in ethanol (100 ml.) was shaken with hydrogen in the presence of a 10% palladium-on-charcoal catalyst (0.6 g.) for 18 hours, filtered and evaporated to dryness. There was thus obtained as residual oil N-n-hexyl-4-methylaminobutyramide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04659516 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-8553b1ced4d744d69d41ee004cc39bf7 |
| Source note | uspto-grants-1987_04 |