HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13931210, compound → HCID 14324147, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13931210 | HCID 13931210 | — |
| Reactant | 5,6-Dimethoxy-2-methyl-3-(2-propyn-1-yl)benzotellurazolium Trifluoromethanesulfonate | HCID 14453425 | — |
| Product | HCID 14324147 | HCID 14324147 | — |
Reaction Steps
This compound was prepared in the same way and on the same scale as the compound of Example 46, except that 5-methoxy-2-methylbenzotellurazole (Example 20) was used in place of the 5,6-dimethoxy-2-methylbenzotellurazole. Yield 1.23 g, 80% of theory, pale tan powder, m.p. 172°-174° C. (dec). The infrared, nuclear magnetic resonance, and mass spectra were in agreement with that expected for the structural formula.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04661438 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-e590e2049cb14a67af53b59b411d852e |
| Source note | uspto-grants-1987_04 |