HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 86741448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | 3-Methoxypropylamine | HCID 1672 | — |
| Reactant | Dimethylphosphite | HCID 21884954 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86741448 | HCID 86741448 | 99.9% |
Reaction Steps
A mixture of 11 g. (0.1 moles) of dimethyl phosphite, 20 ml. of water and 20 ml. of ethanol is reacted with a mixture of 8.51 g. (0.1 moles) of 3-methoxypropyl amine and 30 ml. of methanol as described in Example 1. 18.5 g. of 3-methoxypropyl-ammoniummethyl phosphonate are obtained. Yield: 99.9%. nD30 =1.4449.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04661477 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-3f867465b6544f8b89de31fb49cce87c |
| Source note | uspto-grants-1987_04 |