HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 3-Butyloxypropyl-ammoniummethyl phosphanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1-Propanamine, 3-butoxy- | HCID 85461 | — |
| Reactant | Dimethylphosphite | HCID 21884954 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Butyloxypropyl-ammoniummethyl phosphanate | HCID 86741449 | 89.4% |
Reaction Steps
A mixture of 11 g. (0.1 moles) of dimethyl phosphite, 20 ml. of water and 20 ml. of methanol is reacted with a mixture of 13.12 g. (0.1 moles) of 3-butyloxypropyl amine and 30 ml. of methanol as described in Example 1. 22.6 g. of 3-butyloxypropyl-ammoniummethyl phosphanate are obtained. Yield: 89.4%. nD30 =1.4420
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04661477 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-0c69878de7dc4bf88cc335566ea05459 |
| Source note | uspto-grants-1987_04 |