HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86741451, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 3-Methoxypropylamine | HCID 1672 | — |
| Reactant | Diethylphosphite | HCID 3780918 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86741451 | HCID 86741451 | 94.3% |
Reaction Steps
A mixture of 13.81 g. of diethyl phosphite, 20 ml. of water and 20 ml. of ethanol is reacted with a mixture of 8.91 g. (0.1 moles) of 3-methoxypropyl amine and 30 ml. of ethanol as described in Example 1. 18.8 g. of 3-methoxypropyl-ammoniumethyl phosphanate are obtained. Yield: 94.3%. nD30 =1,4440
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04661477 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-2d6af96cda8844c4b79ed0ef028deb87 |
| Source note | uspto-grants-1987_04 |