HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 20205717, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Cyclopentylamine | HCID 2906 | — |
| Reactant | Diethylphosphite | HCID 3780918 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20205717 | HCID 20205717 | 91.7% |
Reaction Steps
A mixture of 13.81 g. (0.1 moles) of diethyl phosphite, 20 ml. of water and 20 ml. of ethanol is reacted with a mixture of 8.51 g. (0.1 moles) of cyclopentyl amine and 30 ml. of methanol as described in Example 1. 17.9 g. of cyclopentyl-ammoniumethyl phosphonate are obtained. nD30 -1.4622. Yield: 91.7%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04661477 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-979d3eefb4ff494dbc3f9673d99bf7fe |
| Source note | uspto-grants-1987_04 |