HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenoxyethanamine → HCID 14547357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenoxyethanamine | HCID 15651 | — |
| Reactant | N-Benzylaminodiacetic acid | HCID 77606 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 14547357 | HCID 14547357 | 64.8% |
Reaction Steps
2-Phenoxyethylamine (1.37 g) and N-benzyliminodiacetic acid (2.23 g) were mixed and heated to 225°, and maintained at this temperature for 15 min. After cooling, chloroform was added and the product purified by column chromatography (SiO2 /CHCl3) to give the title compound as a reddish oil (2.1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04661489 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-2627d423ca744fcdbd9458e0c850c9e6 |
| Source note | uspto-grants-1987_04 |