HRID543212

反应详情

EQUATION

反应方程式

HRID 543212 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

5 g of 1-(2,3-epoxypropoxy)-4-(2-methoxyethoxy)benzene and 6 g of N-(2-aminoethyl)tetrahydropyran-3-carboxamide are heated together at 130° for 30 minutes. The mixture is allowed to cool and then dissolved in ethyl acetate and worked up in the usual manner. The title compound is obtained (M.P. 107°-108°--from methanol/ethylacetate).

WORKUP

后处理

  1. temperatureto cool