Octylamine → HCID 20206211, compound

Participants

Reaction Steps

2.5 Parts of methyl 5-(2',4'-dihydroxyphenyl)-5-methyl-hexanoate and 5.0 parts of n-octylamine are sealed into a glass Carius tube for 3 days at 120° C. The cooled reaction mixture is taken up in ether, washed first with dilute hydrochloric acid until free of the excess octylamine, and then with water. After removing the ether, the residual oil, on dilution with 40°-60° C. petroleum ether containing a little ether yields 5-(2',4'-dihydroxyphenyl)-5-methyl-hexanoic acid-n-octylamide m.p. 110°-113° C. with the following percentage composition by weight.

Provenance & Evidence