HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylol-alpha-chloroacetamide → HCID 13210257, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylol-alpha-chloroacetamide | HCID 62466 | — |
| Reactant | 4-tert-Butyl-2-(methanesulfonyl)phenol | HCID 12721563 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 13210257 | HCID 13210257 | — |
Reaction Steps
13.5 g (0.06 mol) of 4-(1,1-dimethylethyl)-2-methylsulfonylphenol are dissolved in 100 ml of concentrated sulfuric acid. 6.63 g (0.054 mol) of 2-chloro-N-hydroxymethylacetamide are added and the mixture is stirred at room temperature for 10 minutes. It is then poured onto ice-water and the crude product is filtered off with suction and recrystallized from toluene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04661636 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-9b23d3b4ebcd48de8e478e3ffb461140 |
| Source note | uspto-grants-1987_04 |