HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13210257, compound → HCID 10402160, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13210257 | HCID 13210257 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10402160 | HCID 10402160 | — |
Reaction Steps
6.3 g (0.028 mol) of 2-chloro-N-[5-(1,1-dimethylethyl)-2-hydroxy-3-methylsulfonylbenzyl]acetamide in a mixture of 20 ml of concentrated hydrochloric acid and 40 ml of ethanol are boiled under reflux for 16 hours. The precipitated product is filtered off with suction and recrystallized from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04661636 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-0eec8b5262444e9e87f286f134e53400 |
| Source note | uspto-grants-1987_04 |