HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → 4-(1,1-Dimethylethyl)-2-dimethylaminomethyleneaminosulfonylanisole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 5-(Tert-butyl)-2-methoxybenzenesulfonamide | HCID 10933694 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-(1,1-Dimethylethyl)-2-dimethylaminomethyleneaminosulfonylanisole | HCID 54498328 | — |
Reaction Steps
4.68 g (0.02 mol) of 3-(1,1-dimethylethyl)-6-methoxybenzenesulfonamide are dissolved in 50 ml of dimethylformamide, and 2.5 g (0.022 mol) of dimethylformamide dimethyl acetal are added. The mixture is left at room temperature for 30 minutes, then poured onto ice-water and filtered with suction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04661636 |
| Source dataset | uspto-grants-1987_04 |
| ORD ID | ord-65172e542c3444ca9f6a039737ec3654 |
| Source note | uspto-grants-1987_04 |